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MB Sample ID: SA305814

Local Sample ID:4
Subject ID:SU002935
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606

Select appropriate tab below to view additional metadata details:

Combined analysis:

Analysis ID AN004610 AN004611 AN004612 AN004613
Analysis type MS MS MS MS
Chromatography type HILIC HILIC Reversed phase Reversed phase
Chromatography system Agilent 1290 Agilent 1290 Agilent 1290 Agilent 1290
Column Acquity UPLC BEH Amide column, 2.1 × 100 mm, 1.7 μm Acquity UPLC BEH Amide column, 2.1 × 100 mm, 1.7 μm Agilent Zorbax Eclipse XDB-C18 Rapid Resolution HD 1.8 μm, 2.1 x 100 mm Agilent Zorbax Eclipse XDB-C18 Rapid Resolution HD 1.8 μm, 2.1 x 100 mm
MS Type ESI ESI ESI ESI
MS instrument type QTOF QTOF QTOF QTOF
MS instrument name Agilent 6540 QTOF Agilent 6540 QTOF Agilent 6540 QTOF Agilent 6540 QTOF
Ion Mode POSITIVE NEGATIVE POSITIVE NEGATIVE
Units Area Area Area Area

Chromatography:

Chromatography ID:CH003468
Instrument Name:Agilent 1290
Column Name:Acquity UPLC BEH Amide column, 2.1 × 100 mm, 1.7 μm
Column Temperature:45
Flow Gradient:0–2.5 min: 100% B, 2.5–10 min: 100% B → 0% B; 10–10.01 min: 0% B → 100% B; 10.01–12.5 min: 100% B.
Flow Rate:0.6 mL/min.
Solvent A:50% acetonitrile with 20 mM ammonium formate and 0.25% formic acid, pH 3
Solvent B:90% acetonitrile with 20 mM ammonium formate, 0.25% formic acid, pH 3.
Chromatography Type:HILIC
  
Chromatography ID:CH003469
Instrument Name:Agilent 1290
Column Name:Agilent Zorbax Eclipse XDB-C18 Rapid Resolution HD 1.8 μm, 2.1 x 100 mm
Column Temperature:50
Flow Gradient:2 to 100% B in 10 min; 100% B from 10 min to 14.5 min; 100% to 2% B, from 14.51 min to 16.5 min
Flow Rate:0.4 mL/min.
Solvent A:water with 0.1% (v/v) of formic acid
Solvent B:methanol with 0.1% (v/v) of formic acid
Chromatography Type:Reversed phase
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