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MB Sample ID: SA305793
Local Sample ID: | 8 |
Subject ID: | SU002935 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Species Group: | Mammals |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004610 | AN004611 | AN004612 | AN004613 |
---|---|---|---|---|
Analysis type | MS | MS | MS | MS |
Chromatography type | HILIC | HILIC | Reversed phase | Reversed phase |
Chromatography system | Agilent 1290 | Agilent 1290 | Agilent 1290 | Agilent 1290 |
Column | Acquity UPLC BEH Amide column, 2.1 × 100 mm, 1.7 μm | Acquity UPLC BEH Amide column, 2.1 × 100 mm, 1.7 μm | Agilent Zorbax Eclipse XDB-C18 Rapid Resolution HD 1.8 μm, 2.1 x 100 mm | Agilent Zorbax Eclipse XDB-C18 Rapid Resolution HD 1.8 μm, 2.1 x 100 mm |
MS Type | ESI | ESI | ESI | ESI |
MS instrument type | QTOF | QTOF | QTOF | QTOF |
MS instrument name | Agilent 6540 QTOF | Agilent 6540 QTOF | Agilent 6540 QTOF | Agilent 6540 QTOF |
Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
Units | Area | Area | Area | Area |
Chromatography:
Chromatography ID: | CH003468 |
Instrument Name: | Agilent 1290 |
Column Name: | Acquity UPLC BEH Amide column, 2.1 × 100 mm, 1.7 μm |
Column Temperature: | 45 |
Flow Gradient: | 0–2.5 min: 100% B, 2.5–10 min: 100% B → 0% B; 10–10.01 min: 0% B → 100% B; 10.01–12.5 min: 100% B. |
Flow Rate: | 0.6 mL/min. |
Solvent A: | 50% acetonitrile with 20 mM ammonium formate and 0.25% formic acid, pH 3 |
Solvent B: | 90% acetonitrile with 20 mM ammonium formate, 0.25% formic acid, pH 3. |
Chromatography Type: | HILIC |
Chromatography ID: | CH003469 |
Instrument Name: | Agilent 1290 |
Column Name: | Agilent Zorbax Eclipse XDB-C18 Rapid Resolution HD 1.8 μm, 2.1 x 100 mm |
Column Temperature: | 50 |
Flow Gradient: | 2 to 100% B in 10 min; 100% B from 10 min to 14.5 min; 100% to 2% B, from 14.51 min to 16.5 min |
Flow Rate: | 0.4 mL/min. |
Solvent A: | water with 0.1% (v/v) of formic acid |
Solvent B: | methanol with 0.1% (v/v) of formic acid |
Chromatography Type: | Reversed phase |