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MB Sample ID: SA299859

Local Sample ID:20210311-35Gy-4-5-120h
Subject ID:SU002901
Subject Type:Mammal
Subject Species:Rattus norvegicus
Gender:Female

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Combined analysis:

Analysis ID AN004545 AN004546
Analysis type MS MS
Chromatography type Reversed phase Reversed phase
Chromatography system Thermo TSQ Vantage HPLC-MS/MS Thermo TSQ Vantage HPLC-MS/MS
Column Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um) Waters ACQUITY UPLC BEH C8 (100 x 2.1mm,1.7um)
MS Type ESI ESI
MS instrument type Triple quadrupole Triple quadrupole
MS instrument name Thermo TSQ Vantage Thermo TSQ Vantage
Ion Mode NEGATIVE POSITIVE
Units peak area peak area

Chromatography:

Chromatography ID:CH003414
Chromatography Summary:negtive ion mode
Instrument Name:Thermo TSQ Vantage HPLC-MS/MS
Column Name:Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um)
Column Temperature:55
Flow Gradient:0~1 min, 2% B; 1-20 min, 2~100% B; 20~24min, 100% B; 24~24.5min, 100~2% B; 24.5~34 min, 2% B
Flow Rate:0.35 mL/min
Solvent A:100% water; 0.1% formic acid
Solvent B:100% acetonitrile; 0.1% formic acid
Chromatography Type:Reversed phase
  
Chromatography ID:CH003415
Chromatography Summary:positive ion mode
Instrument Name:Thermo TSQ Vantage HPLC-MS/MS
Column Name:Waters ACQUITY UPLC BEH C8 (100 x 2.1mm,1.7um)
Column Temperature:50
Flow Gradient:0~0.5min, 5% B; 0.5 ~24min, 5~100% B; 24-28 min, 40-100% B; 28~28.5min, 100~5% B; 28.5~48 min, 5% B
Flow Rate:0.35 mL/min
Solvent A:water(0.1% formic acid )
Solvent B:acetonitrile(0.1% formic acid )
Chromatography Type:Reversed phase
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